New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
The objective of this subject is to introduce the undergraduate students with the most important separation equipments in the process industry, and provide proper understanding of unit operations. At the end of study the student will come to know basic operations of cooling towers, dryer, as well as design of a adsorber and calculations involved in liquid-liquid extraction and solid liquid extraction.
Mc-Cabe, W.L. Smith J.M. – Unit Operation in Chemical Engg.,5th edition Tata McGraw Hill Hogakusha, Tokyo, New Delhi.
Coulson J.M. Richardson J.F.-Chemical Engg., Vol 2, Edition-2, Butserworth Heinmann, Oxford, New Delhi.
Treybal R.E. – Mass Transfer Operation – 3rd edition, Mc. Graw Hill Book Co. New York.
To study the rate dissolution of a rotating cylinder and then to calculate the mass transfer coefficient.
Study of Adsorption in a packed bed for a Solid liquid system, plotting the breakthrough curve of adsorption for a given system
To study the performance of forced draft water-cooling tower.
To study the drying characteristics of a wet granular material using natural and forced circulation in tray dryer.
Studies on solid-liquid extraction column.
To study the yield of crystals of a saturated solution using open tank type agitated batch crystallizer.
To study the yield of crystals of a saturated solution using Swenson walker crystallizer.
To draw the tie lines and plot equilibrium curve for given ternary system.
Liquid- Liquid extraction in a packed column for co-current and counter current flow of binary systems.
To Study on Liquid-Liquid extraction on a spray Extraction Column.
New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
reaction rate.
Unit-IV Design of catalytic reactors : Isothermal & adiabatic fixed bad reactor staged adiabatic reactors, Non isothermal, non adiabatic fixed bed reactors, Fluidized bed reactors, Slurry reactors, Trickle bed reactors.
Unit-V Models and Regime for Fluids : Solid non-catalytic reactions, controlling mechanisms, Diffusion through gas film controls. Diffusion through ash layer controls, Chemical reaction controls, fluidized bed reactors with and without elutriation. Gas-liquid reactions and liquid-liquid reaction, Rate equation based on film theory, Reaction design for instantaneous reactions and slow reactions, Aerobic Fermentation, Application to Design Tools for Fast Reactions.
Smith J.M; Chemical Engineering Kinetics; Mc Graw Hill.
Denbigh & Turner K.G; Chemical Reaction Theory an Introduction; United Press.
Copper & Jeffery’s GVJ; Chemical Kinetics and Reactor Engineering; Prentice Hall
Levenspiel O; Chemical Reaction Engg; Willey Eastern, Singapore.
Houghen Watson & Ragatz; Chemical Process Principles Part Iii; Asian Pub-House Mumbai
Fogler H.S; Elements of Chemical Reaction Engineering; PHI
To determine velocity rate constant of the hydrolysis of ethyl acetate by sodium hydroxide.
To study the rate constant of hydrolysis of an ester-catalyzed by acid.
Determine the rate constant and order of reaction between Potassium per sulphate and potassium iodide.
To study temperature dependency of rate constant, evaluation of activation energy and verification of Arrhenius law.
To study a consecutive reaction system (hydraulic model).
To study a parallel reaction system (hydraulic model).
To study a homogeneous reaction in a semi-batch reactor under isothermal conditions.
Study of non catalytic homogeneous saponification reaction in CSTR.
To study a non-catalytic homogeneous reaction in a plug flow reactor.
To study the residence time distribution behavior of a back mix reactor.
To study the RTD behavior of a tubular reactor.
To study the RTD behavior of a packed bed reactor.
To study the behavior of a continuous flow reactor system-three reactor in series.
To study the kinetics of thermal decomposition of calcium carbonate.
To study a homogeneous catalytic reaction in a batch reactor under adiabatic conditions.
Study of non catalytic saponification reaction in a tubular flow reactor.
The objective of this course is to acquire basic understanding of design parameter, complete knowledge of design procedures for commonly used process equipment and their attachments (e.g. internal and external pressure vessels, tall vessels, high pressure vessels, supports etc.), and different types of equipment testing methods.
Brownell, N.E and Young, H.E; Process Equipment Design; John Wiley
Bhattacharya, B.C; Introduction of Chemical Equipment Design; CBS Publishers, Delhi.
Perry RH; Hand book of Chemical Engg; Mc Graw Hill Pub
I.S.: 2825-1969 – Code For Unfired Pressure Vessels.
I.S. 803-1962, Code for Practice for Design, Fabrication and Erection of Vertical and Mild Steel Cylindrical Welded Oil Storage Tanks.
Joshi, M.V.; Process Equipment Design.
Ludwig EE; Applied Process Design in Chemical and Petrochemical
Chain, step and miscellaneous polymerization reactions and polymerization technique. Polymerization kinetics: Free radical, cationic and anionic polymerization, poly-condensation and polymerization.
Bulk solution, emulsion and suspension polymerization, thermoplastic composites, fiber reinforcement fillers, surface treatment reinforced thermo-set composites resins, fillers, additives.
Hydrolysis, acidolysis, aminolysis, hydrogenation, addition and substitution reactions, reactions of various specific groups, cyclization and cross linking reactions, reactions leading to graft and block copolymer
Plastics- polyethylene, polypropylene polyvinyl chloride & copolymer, polystyrene; Phenol- formaldehyde, epoxides, urethane, Teflon, elastomers, robbers, polymeric oils - silicon fibers - cellulosic (Rayon), polyamides (6:6 Nylon), Polyesters (Dacron). Acrylic-olefin.
Ceramic and other fiber reinforced plastics, Polymer degradation - Thermal, Mechanical, Ultrasonic, Photo, High energy radiation, Ecology and environmental aspects of polymer industries. Rheological Sciences Equations, Uni-coelastic models - Maxwell.
Rodringuez; Principles of polymer systems; TMH
Billmayer Jr, Fred W.; Textbook of polymer science; Wiley tappon
David J Williams; Polymer science & engineering; PHI
Mc. Keley, JH; Polymer processing; John Wiley
Definition and examples of the main intermolecular forces and in supramolecular chemistry.
Self-assembly process in organic systems. Main supramolecular structures.
Students will be exposed to the very basics of nanomaterial; A series of nonmaterial that exhibit unique properties will be introduced.
Methods of Synthesis of Nonmaterial. Equipment and processes needed to fabricate nano devices and structures such as bio-chips, power devices, and opto-electronic structures. Bottom-up (building from molecular level) and top-down (breakdown of microcrystalline materials) approaches.
Biologically- Inspired Nanotechnology, basic biological concepts and principles that may lead to the development of technologies for nano engineering systems. Coverage will be given to how life has evolved sophisticatedly, molecular nano scale engineered devices, and discuss how these nano scale biotechnologies are far more elaborate in their functions than most products made by humans.
Instrumentation for nano scale Characterization. Instrumentation required for characterization of properties on the nano meter scale. The measurable properties and resolution limits of each technique, with an emphasis on measurements in the nano meter range.
Supramolecular Chemistry by Jean-Maric Lehn,
Supramolecular Chemistry by Jonathan Steel & Jerry Atwood
Intermolecular and Surface Forces by Jacob Israelachvili.
The objective this course enables the students to know about control methods and make the students knowledgeable in various types of measuring instruments used in chemical process industries.
Coughnower & Koppel – Process System Analysis and Control- McGraw Hill, New York.
D. P. Eckman – Automatics Process Control – McGraw Hill, New York.
Peter Harriot – Process Control – McGraw Hill, New York.
J. J. Nagrath & M. Gopal; Control System Engineering.
Formulation of the objective function. Unconstrained single variable optimization: Newton, Quasi- Newton methods, polynomial approximation methods.
Unconstrained multivariable optimization: Direct search method, conjugate search method, steepest descent method, conjugate gradient method, Newton’s method.
Linear Programming: Formulation of LP problem, graphical solution of LP problem, simplex method, duality in Linear Programming, two-phase method.
Non linear programming with constraints: Necessary and sufficiency conditions for a local extremum, Quadratic programming, successive quadratic programming, Generalized reduced gradient (GRG) method.
Applications of optimization in Chemical Engineering.
Edgar, T.F., Himmelblau, D. M., Lasdon, L. S., “Optimization of Chemical Process”, 2nd ed. McGraw- Hill, 2001.
Rao, S. S., “Optimisation Techniques”, Wiley Eastern, New Delhi, 1985.
Gupta, S. K., “Numerical Methods for Engineers”, New Age, 1995.
Beveridge, G. S. and Schechter, R. S., “Optimization Theory and Practice”, McGraw- Hill, New York,1970.
Rekllaitis, G.V., Ravindran, A. and Ragsdell, K. M., “Engineering Optimization- Methods and Applications”, John Wiley, New York, 1983
New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
To Study of organic process industries involving process technology, raw material availability, production pattern, Engg. problems involving material of construction, Environment pollution, waste utilization and disposal, energy consumption and conservation Equation.
Plant nutrients, different types of fertilizers and their production in India. Different feed stocks. Synthesis gas production by steam-naphtha reforming and gas purification. Ammonia synthesis.
Urea manufacturing processes. Manufacture of sulphuric acid and ammonium sulphate. Nitric acid and ammonium nitrate manufacture.
Availability and grinding of rock phosphate, manufacturing processes for single and triple super- phosphate and phosphoric acid.
Availability and manufacture of muriate of potash. Mono and di-ammonium phosphate, urea ammonium phosphates, NPK complex fertilizers, granulation techniques.
Fertilizers storage and handling. Corrosion problems in fertilizers industries, Fertilizer plant effluent treatment and disposal.
Slack A.V. “Chemistry and Technology of Fertilizers”, Wiley interscience Publishers.
Waggaman W.H., “Phosphoric Acid, Phosphates and Phosphatic Fertilizers”, Hafner Pub.
Austin G.T., “Shreve’s Chemical Processes Industries”, 5th Ed. McGraw Hill.
Rao M.G. and Sittig M., “Dryden’s Outlines of Chemical Technology”, Affiliated East W Press, Delhi.
Simulation Study of Various Chemical Process with the help of following Softwares :
Introduction to Polymath software: Understanding its function & working.
Prodyn: Understanding its functions & working.
Practical exercise using MATLAB, CHEMCAD & Prosimulator.
To study the characteristics of control valves (linear, quick opening, etc)
To study the dynamics of liquid level systems of non-interacting and interacting types.
To study the response of mercury in glass thermometer with and without a thermowell.
To study the characteristics of an electronic PID controller.
To study the characteristics of a current to pneumatic converter.
To study the effectiveness of computer control of a distillation column.
To study the effectiveness of a computer control of a heat exchanger.
To study to effectiveness of a computer control of a chemical reactor
To study to dynamics of a pressure tanks.
To calibrate an air purged liquid level indicator.
New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
The objective of this subject is to introduce the undergraduate students with the most important separation equipments in the process industry, and provide proper understanding of unit operations. At the end of study the student will come to know basic operations of cooling towers, dryer, as well as design of a adsorber and calculations involved in liquid-liquid extraction and solid liquid extraction.
Mc-Cabe, W.L. Smith J.M. – Unit Operation in Chemical Engg.,5th edition Tata McGraw Hill Hogakusha, Tokyo, New Delhi.
Coulson J.M. Richardson J.F.-Chemical Engg., Vol 2, Edition-2, Butserworth Heinmann, Oxford, New Delhi.
Treybal R.E. – Mass Transfer Operation – 3rd edition, Mc. Graw Hill Book Co. New York.
To study the rate dissolution of a rotating cylinder and then to calculate the mass transfer coefficient.
Study of Adsorption in a packed bed for a Solid liquid system, plotting the breakthrough curve of adsorption for a given system
To study the performance of forced draft water-cooling tower.
To study the drying characteristics of a wet granular material using natural and forced circulation in tray dryer.
Studies on solid-liquid extraction column.
To study the yield of crystals of a saturated solution using open tank type agitated batch crystallizer.
To study the yield of crystals of a saturated solution using Swenson walker crystallizer.
To draw the tie lines and plot equilibrium curve for given ternary system.
Liquid- Liquid extraction in a packed column for co-current and counter current flow of binary systems.
To Study on Liquid-Liquid extraction on a spray Extraction Column.
New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
reaction rate.
Unit-IV Design of catalytic reactors : Isothermal & adiabatic fixed bad reactor staged adiabatic reactors, Non isothermal, non adiabatic fixed bed reactors, Fluidized bed reactors, Slurry reactors, Trickle bed reactors.
Unit-V Models and Regime for Fluids : Solid non-catalytic reactions, controlling mechanisms, Diffusion through gas film controls. Diffusion through ash layer controls, Chemical reaction controls, fluidized bed reactors with and without elutriation. Gas-liquid reactions and liquid-liquid reaction, Rate equation based on film theory, Reaction design for instantaneous reactions and slow reactions, Aerobic Fermentation, Application to Design Tools for Fast Reactions.
Smith J.M; Chemical Engineering Kinetics; Mc Graw Hill.
Denbigh & Turner K.G; Chemical Reaction Theory an Introduction; United Press.
Copper & Jeffery’s GVJ; Chemical Kinetics and Reactor Engineering; Prentice Hall
Levenspiel O; Chemical Reaction Engg; Willey Eastern, Singapore.
Houghen Watson & Ragatz; Chemical Process Principles Part Iii; Asian Pub-House Mumbai
Fogler H.S; Elements of Chemical Reaction Engineering; PHI
To determine velocity rate constant of the hydrolysis of ethyl acetate by sodium hydroxide.
To study the rate constant of hydrolysis of an ester-catalyzed by acid.
Determine the rate constant and order of reaction between Potassium per sulphate and potassium iodide.
To study temperature dependency of rate constant, evaluation of activation energy and verification of Arrhenius law.
To study a consecutive reaction system (hydraulic model).
To study a parallel reaction system (hydraulic model).
To study a homogeneous reaction in a semi-batch reactor under isothermal conditions.
Study of non catalytic homogeneous saponification reaction in CSTR.
To study a non-catalytic homogeneous reaction in a plug flow reactor.
To study the residence time distribution behavior of a back mix reactor.
To study the RTD behavior of a tubular reactor.
To study the RTD behavior of a packed bed reactor.
To study the behavior of a continuous flow reactor system-three reactor in series.
To study the kinetics of thermal decomposition of calcium carbonate.
To study a homogeneous catalytic reaction in a batch reactor under adiabatic conditions.
Study of non catalytic saponification reaction in a tubular flow reactor.
The objective of this course is to acquire basic understanding of design parameter, complete knowledge of design procedures for commonly used process equipment and their attachments (e.g. internal and external pressure vessels, tall vessels, high pressure vessels, supports etc.), and different types of equipment testing methods.
Brownell, N.E and Young, H.E; Process Equipment Design; John Wiley
Bhattacharya, B.C; Introduction of Chemical Equipment Design; CBS Publishers, Delhi.
Perry RH; Hand book of Chemical Engg; Mc Graw Hill Pub
I.S.: 2825-1969 – Code For Unfired Pressure Vessels.
I.S. 803-1962, Code for Practice for Design, Fabrication and Erection of Vertical and Mild Steel Cylindrical Welded Oil Storage Tanks.
Joshi, M.V.; Process Equipment Design.
Ludwig EE; Applied Process Design in Chemical and Petrochemical
Chain, step and miscellaneous polymerization reactions and polymerization technique. Polymerization kinetics: Free radical, cationic and anionic polymerization, poly-condensation and polymerization.
Bulk solution, emulsion and suspension polymerization, thermoplastic composites, fiber reinforcement fillers, surface treatment reinforced thermo-set composites resins, fillers, additives.
Hydrolysis, acidolysis, aminolysis, hydrogenation, addition and substitution reactions, reactions of various specific groups, cyclization and cross linking reactions, reactions leading to graft and block copolymer
Plastics- polyethylene, polypropylene polyvinyl chloride & copolymer, polystyrene; Phenol- formaldehyde, epoxides, urethane, Teflon, elastomers, robbers, polymeric oils - silicon fibers - cellulosic (Rayon), polyamides (6:6 Nylon), Polyesters (Dacron). Acrylic-olefin.
Ceramic and other fiber reinforced plastics, Polymer degradation - Thermal, Mechanical, Ultrasonic, Photo, High energy radiation, Ecology and environmental aspects of polymer industries. Rheological Sciences Equations, Uni-coelastic models - Maxwell.
Rodringuez; Principles of polymer systems; TMH
Billmayer Jr, Fred W.; Textbook of polymer science; Wiley tappon
David J Williams; Polymer science & engineering; PHI
Mc. Keley, JH; Polymer processing; John Wiley
Definition and examples of the main intermolecular forces and in supramolecular chemistry.
Self-assembly process in organic systems. Main supramolecular structures.
Students will be exposed to the very basics of nanomaterial; A series of nonmaterial that exhibit unique properties will be introduced.
Methods of Synthesis of Nonmaterial. Equipment and processes needed to fabricate nano devices and structures such as bio-chips, power devices, and opto-electronic structures. Bottom-up (building from molecular level) and top-down (breakdown of microcrystalline materials) approaches.
Biologically- Inspired Nanotechnology, basic biological concepts and principles that may lead to the development of technologies for nano engineering systems. Coverage will be given to how life has evolved sophisticatedly, molecular nano scale engineered devices, and discuss how these nano scale biotechnologies are far more elaborate in their functions than most products made by humans.
Instrumentation for nano scale Characterization. Instrumentation required for characterization of properties on the nano meter scale. The measurable properties and resolution limits of each technique, with an emphasis on measurements in the nano meter range.
Supramolecular Chemistry by Jean-Maric Lehn,
Supramolecular Chemistry by Jonathan Steel & Jerry Atwood
Intermolecular and Surface Forces by Jacob Israelachvili.
The objective this course enables the students to know about control methods and make the students knowledgeable in various types of measuring instruments used in chemical process industries.
Coughnower & Koppel – Process System Analysis and Control- McGraw Hill, New York.
D. P. Eckman – Automatics Process Control – McGraw Hill, New York.
Peter Harriot – Process Control – McGraw Hill, New York.
J. J. Nagrath & M. Gopal; Control System Engineering.
Formulation of the objective function. Unconstrained single variable optimization: Newton, Quasi- Newton methods, polynomial approximation methods.
Unconstrained multivariable optimization: Direct search method, conjugate search method, steepest descent method, conjugate gradient method, Newton’s method.
Linear Programming: Formulation of LP problem, graphical solution of LP problem, simplex method, duality in Linear Programming, two-phase method.
Non linear programming with constraints: Necessary and sufficiency conditions for a local extremum, Quadratic programming, successive quadratic programming, Generalized reduced gradient (GRG) method.
Applications of optimization in Chemical Engineering.
Edgar, T.F., Himmelblau, D. M., Lasdon, L. S., “Optimization of Chemical Process”, 2nd ed. McGraw- Hill, 2001.
Rao, S. S., “Optimisation Techniques”, Wiley Eastern, New Delhi, 1985.
Gupta, S. K., “Numerical Methods for Engineers”, New Age, 1995.
Beveridge, G. S. and Schechter, R. S., “Optimization Theory and Practice”, McGraw- Hill, New York,1970.
Rekllaitis, G.V., Ravindran, A. and Ragsdell, K. M., “Engineering Optimization- Methods and Applications”, John Wiley, New York, 1983
New Scheme Based On AICTE Flexible Curricula Chemical Engineering, VI-Semester
To Study of organic process industries involving process technology, raw material availability, production pattern, Engg. problems involving material of construction, Environment pollution, waste utilization and disposal, energy consumption and conservation Equation.
Plant nutrients, different types of fertilizers and their production in India. Different feed stocks. Synthesis gas production by steam-naphtha reforming and gas purification. Ammonia synthesis.
Urea manufacturing processes. Manufacture of sulphuric acid and ammonium sulphate. Nitric acid and ammonium nitrate manufacture.
Availability and grinding of rock phosphate, manufacturing processes for single and triple super- phosphate and phosphoric acid.
Availability and manufacture of muriate of potash. Mono and di-ammonium phosphate, urea ammonium phosphates, NPK complex fertilizers, granulation techniques.
Fertilizers storage and handling. Corrosion problems in fertilizers industries, Fertilizer plant effluent treatment and disposal.
Slack A.V. “Chemistry and Technology of Fertilizers”, Wiley interscience Publishers.
Waggaman W.H., “Phosphoric Acid, Phosphates and Phosphatic Fertilizers”, Hafner Pub.
Austin G.T., “Shreve’s Chemical Processes Industries”, 5th Ed. McGraw Hill.
Rao M.G. and Sittig M., “Dryden’s Outlines of Chemical Technology”, Affiliated East W Press, Delhi.
Simulation Study of Various Chemical Process with the help of following Softwares :
Introduction to Polymath software: Understanding its function & working.
Prodyn: Understanding its functions & working.
Practical exercise using MATLAB, CHEMCAD & Prosimulator.
To study the characteristics of control valves (linear, quick opening, etc)
To study the dynamics of liquid level systems of non-interacting and interacting types.
To study the response of mercury in glass thermometer with and without a thermowell.
To study the characteristics of an electronic PID controller.
To study the characteristics of a current to pneumatic converter.
To study the effectiveness of computer control of a distillation column.
To study the effectiveness of a computer control of a heat exchanger.
To study to effectiveness of a computer control of a chemical reactor
To study to dynamics of a pressure tanks.
To calibrate an air purged liquid level indicator.